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HRID2181351

反应详情

EQUATION

反应方程式

HRID 2181351 的结构方程式

REACTANTS

反应物

2
结构：C=CC(C)(C)O
HCID8257

2-Methyl-3-buten-2-ol

C5H10O

结构：CC(C)Cn1c(=O)n(C)c(=O)c2c(Br)c(Cc3ccccc3C(F)(F)F)sc21
HCID11442902

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Cn1c(=O)n(C)c(=O)c2c(C=CC(C)(C)O)c(Cc3ccccc3C(F)(F)F)sc21
HCID69746621

未命名化合物

PROCEDURE

实验过程

Prepared using 5-bromo-3-methyl-1-(2-methylpropyl)-6-[[2-(trifluoromethyl)phenyl]methyl]-thieno[2,3-d]pyrimidine-2,4(1H,3H)-dione and 2-methyl-3-buten-2-ol. The crude product was purified by flash silica chromatography eluting with a gradient of 0-2% ethanol in dichloromethane to give the title compound as a cream foam (0.20 g).

WORKUP

后处理

  1. customPrepared
  2. customThe crude product was purified by flash silica chromatography
  3. washeluting with a gradient of 0-2% ethanol in dichloromethane