HRID2181352

反应详情

EQUATION

反应方程式

HRID 2181352 反应方程式

PROCEDURE

实验过程

Prepared using 5-bromo-3-methyl-1-(2-methylpropyl)-6-[[2-(trifluoromethyl)phenyl]methyl]-thieno[2,3-d]pyrimidine-2,4(1H,3H)-dione and cyclopentyl-ethene. The crude product was purified by flash silica chromatography eluting with a gradient of 5-20% ethanol in dichloromethane to give the title compound as a yellow oil (0.17 g).

WORKUP

后处理

  1. customPrepared
  2. customThe crude product was purified by flash silica chromatography
  3. washeluting with a gradient of 5-20% ethanol in dichloromethane