HRID2181587

反应详情

EQUATION

反应方程式

HRID 2181587 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 4-bromo-2,5-xylidine (8 g) in pyridine (60 ml) was added pivaloyl chloride (4.7 ml) at room temperature. After 30 minutes, the mixture was poured into dilute hydrochloric acid/ice solution. The precipitate was filtered and washed with water to give the title product.

WORKUP

后处理

  1. filtrationThe precipitate was filtered
  2. washwashed with water