HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,2-Trifluoroethanesulfonyl chloride → HCID 59251192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,2-Trifluoroethanesulfonyl chloride | HCID 74242 | — |
| Reactant | HCID 86640192 | HCID 86640192 | — |
| Product | HCID 59251192 | HCID 59251192 | 99.7% |
Reaction Steps
Prepared from 3-(1-(4-fluorophenyl)-1H-indazol-5-yl)-3-phenylpropan-1-amine TFA salt (25 mg, 0.05 mmol) by adding 2,2,2-trifluoroethanesulfonyl chloride under the General Coupling Method B conditions. Obtained 22 mg (82%) of 2,2,2-trifluoro-N-(3-(1-(4-fluorophenyl)-1H-indazol-5-yl)-3-phenylpropyl)acetamide. MS found: (M+H)+=442.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198311B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-a01969a549c042219f0cc70650620c13 |
| Source note | uspto-grants-2012_06 |