1,3-Benzenedimethanamine → HCID 86593943, compound

Participants

Reaction Conditions

Reaction Steps

To a stirred suspension of galactaric acid (5.004 g, 23.811 mmol) in deionized water (50.0 mL), m-xylylenediamine (3.15 mL, 23.868 mmol) was added using a pipette. The reaction mixture was stirred at 70° C. for 16 h. The reaction mixture was filtered, washed with several small portions of deionized water, and then dried under vacuum at room temperature for 24 h to give white solid, m-xylylenediammonium galactarate 14, 6.016 g, 17.372 mmol, 72.88%).

Provenance & Evidence