Potassium Carbonate → 3-Chloro-5-[(4-methoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridine

Participants

Reaction Steps

The title compound was prepared from N-[1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethyl]-4-methoxybenzenesulfonamide (617 mg, 1.5 mmol), anhydrous N,N-dimethylformamide (2 mL), and potassium carbonate (414 mg, 3.0 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 607 mg (93%) of a white solid that was used without further purification;

Provenance & Evidence