HRID2181931

反应详情

EQUATION

反应方程式

HRID 2181931 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared from N-[1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethyl]-4-methoxybenzenesulfonamide (617 mg, 1.5 mmol), anhydrous N,N-dimethylformamide (2 mL), and potassium carbonate (414 mg, 3.0 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 607 mg (93%) of a white solid that was used without further purification;