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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2181932Generated: October 31, 2026

Triethylamine → HCID 22482374, compound

https://huagongshe.com/reaction/2181932

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant2,4-Dimethoxybenzenesulfonyl chlorideHCID 2734626—
Reactant1-(4'-Chloro-2'-fluoro-biphenyl-2-yl)-ethylamineHCID 22482361—
ProductHCID 22482374HCID 22482374—

Reaction Steps

The title compound was prepared from 2,4-dimethoxybenzenesulfonyl chloride (379 mg, 1.6 mmol), 1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethylamine (400 mg, 1.6 mmol), and triethylamine (246 μL, 1.7 mmol) according to the procedure and in the same manner as described in Example 105, step c resulting in the isolation of 480 mg (67%) of a white solid;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06894061B2
Source datasetuspto-grants-2005_05
ORD IDord-ee093dd17c7f4366b940b04a008c5b02
Source noteuspto-grants-2005_05