HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22482374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,4-Dimethoxybenzenesulfonyl chloride | HCID 2734626 | — |
| Reactant | 1-(4'-Chloro-2'-fluoro-biphenyl-2-yl)-ethylamine | HCID 22482361 | — |
| Product | HCID 22482374 | HCID 22482374 | — |
Reaction Steps
The title compound was prepared from 2,4-dimethoxybenzenesulfonyl chloride (379 mg, 1.6 mmol), 1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethylamine (400 mg, 1.6 mmol), and triethylamine (246 μL, 1.7 mmol) according to the procedure and in the same manner as described in Example 105, step c resulting in the isolation of 480 mg (67%) of a white solid;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06894061B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-ee093dd17c7f4366b940b04a008c5b02 |
| Source note | uspto-grants-2005_05 |