HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10772367, compound → HCID 9811548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10772367 | HCID 10772367 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 9811548 | HCID 9811548 | — |
Reaction Steps
A solution of 5 mmol of the product obtained in Example 1 in 25 ml of hydrogen chloride-saturated dioxane is stirred for 20 minutes at 20° C. The whole mixture is concentrated under vacuum and the residue is washed with pentane, to give the expected product in hydrochloride form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05424464 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-82bd3a41a9f147679decbb201340163b |
| Source note | uspto-grants-1995_06 |