HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22482760, compound → HCID 12069438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22482760 | HCID 22482760 | — |
| Solvent | Sodium Bicarbonate | HCID 516892 | — |
| Product | HCID 12069438 | HCID 12069438 | — |
Reaction Steps
5-carbamoyl-1,2,3,6-tetrahydropyridine hydrochloride was dissolved in a saturated aqueous solution of sodium hydrogen carbonate, followed by extraction with chloroform. The organic layer was dried over anhydrous sodium sulfate. After the desiccant was filtered off, the filtrate was concentrated under reduced pressure to yield crystals of free 5-carbamoyl-1,2,3,6-tetrahydropyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06894168B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-4e7c079827854e52b37e0f29ff0eb8f4 |
| Source note | uspto-grants-2005_05 |