HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86588635, compound → HCID 22482058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86588635 | HCID 86588635 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 22482058 | HCID 22482058 | — |
Reaction Steps
A solution of 5′-bromo-6′-(3-chloro-benzyloxy)-3,4,5,6-tetrahydro-2H-[1,2′]bipyrazinyl-4-carboxylic acid tert-butyl ester I-3j (25 mg, 0.052 mmol) in formic acid (96%, 0.75 ml) was stirred at room temperature for 2 h, and concentrated in vacuo. The title compound 3-R was collected as a white solid (26 mg, >99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06894050B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-9a652b6ab6fa426e817e3ea7ec8e3c6d |
| Source note | uspto-grants-2005_05 |