HuagongsheHuagongshe Chemistry Print Report · For research reference only
Semicarbazide hydrochloride → Ethyl pyruvate semicarbazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Semicarbazide hydrochloride | HCID 11236 | — |
| Reactant | Ethyl pyruvate | HCID 12041 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Water | HCID 962 | — |
| Product | Ethyl pyruvate semicarbazide | HCID 22477923 | — |
Reaction Steps
A stirred solution of semicarbazide hydrochloride (11.1 g) and sodium acetate (8.2 g) in water (250 ml) was treated with ethyl pyruvate (10.9 ml) in one portion. The resulting white precipitate was collected by filtration to yield ethyl pyruvate semicarbazide (16.59 g) as a white powder. LC-MS (Method J): RT=2.38 minutes, 174.31 (M+H)+, 172.32 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06897208B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-10ff88b54fb44e3e837b0a0ecc9e3b1b |
| Source note | uspto-grants-2005_05 |