HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 22480359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | HCID 15408136 | HCID 15408136 | — |
| Product | HCID 22480359 | HCID 22480359 | — |
Reaction Steps
200 mg (0.6 mmol) of 1-benzyl-3-(5-ethoxycarbonyl-2-furyl)indazole were dissolved in ethylene glycol and heated under reflux for 1.5 h. For work-up, the mixture was concentrated using a rotary evaporator and the crude product was chromatographed over silica gel using hexane/ethyl acetate (1:1). This gave 68 mg (31%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06897232B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-274786430a4441f3b6bbd602bdcc8918 |
| Source note | uspto-grants-2005_05 |