Isopropyl iodide → HCID 22479275, compound

Participants

Reaction Steps

2-Iodopropane (0.5 ml) was added to a suspension of Example 196 (0.17 g) and CS2CO3 (0.28 g) in DMF (3 mL) and the mixture was stirred for 4 hours. The mixture was diluted with citric acid and the solution was extracted with EtOAc. EtOAc layer was washed with water and brine, dried and evaporated. The residue was purified via HPLC to yield the titled compound (0.13 g). MS m/z 435(MH+).

Provenance & Evidence