HCID 10215510, compound → Hydrochloric Acid

Participants

Reaction Steps

By the method of Procedure 7 substituting (4-chlorophenyl)-[4-(hydroxypyridin-4-yl-methyl )-1,3,5-trimethyl-1H-pyrrol-2-yl]-methanone for 5-[[2-(4-chlorobenzoyl)-1-methyl-1H-pyrrol-4-yl]carbonyl]-3-(triphenylmethyl)-1H-imidazolium the title compound was prepared. Treatment with ethereal HCl gave 35% yield of the hydrochloride salt. Mp. 174-176° C. ES-MS m/z=353 (M++H). 1HNMR (CDCl3) δ 8.9 (ar, 2H); 8 (ar, 2H); 7.7 (ar, 2H); 7.5 (ar, 2H); 3.75 (s, 3H); 2.3 (s, 3H); 2.65 (s, 3H).

Provenance & Evidence