HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2,5-difluorobenzonitrile → [3-(5-Chloro-2-cyano-4-fluorophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2,5-difluorobenzonitrile | HCID 11275302 | — |
| Reactant | 1,1-Dimethylethyl (3-hydroxypentyl)methylcarbamate | HCID 85790425 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | [3-(5-Chloro-2-cyano-4-fluorophenoxy)pentyl]methylcarbamic acid, 1,1-dimethylethyl ester | HCID 91069775 | — |
Reaction Steps
The subtitle compound was prepared according to the method of Example 3 step (b) using (3-hydroxypentyl)methylcarbamic acid, 1,1-dimethylethyl ester and 4-chloro-2,5-difluorobenzonitrile in N,N-dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900243B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-786396e702c94e1e93c4348ce895536a |
| Source note | uspto-grants-2005_05 |