4-Chloro-2-fluoro-1-nitrobenzene → HCID 86587543, compound

HRID 2183849Notes

Reaction equation

HRID 2183849 reaction equation
[OH:1][CH:2]([CH2:14][CH2:15][CH3:16])[CH2:3][CH2:4][N:5]([CH3:13])[C:6](=[O:12])[O:7][C:8]([CH3:11])([CH3:10])[CH3:9].[Cl:17][C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[C:20](F)[CH:19]=1>CN(C)C=O>[CH3:9][C:8]([O:7][C:6](=[O:12])[N:5]([CH2:4][CH2:3][CH:2]([O:1][C:22]1[CH:23]=[C:18]([Cl:17])[CH:19]=[CH:20][C:21]=1[N+:24]([O-:26])=[O:25])[CH2:14][CH2:15][CH3:16])[CH3:13])([CH3:10])[CH3:11]

Participants

4

Reactant 2

HCID 696914-Chloro-2-fluoro-1-nitrobenzeneHCID 85790426HCID 85790426, compound

Product 1

HCID 86587543HCID 86587543, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The subtitle compound was prepared according to the method of Example 3 step (b) using (3-hydroxyhexyl)methylcarbamic acid, 1,1-dimethylethyl ester and 4-chloro-2-fluoronitrobenzene in N,N-dimethylformamide.

Sources & evidence

ORD record
ord-cb3cbbe6cebe46fb828fb70ed65f1dbd
Source dataset
uspto-grants-2005_05
Patent number
US06900243B2

Reaction notes

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