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HRID2184081

反应详情

EQUATION

反应方程式

HRID 2184081 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)CN(C)c1ccccc1
HCID265936

Ethyl N-methyl-N-phenylglycinate

C11H15NO2

结构：CCOC(=O)CN(C)c1ccc(C(O)(C(F)(F)F)C(F)(F)F)cc1
HCID10406140

未命名化合物

PRODUCTS

生成物

1
结构：CN(CCO)c1ccccc1
HCID62340

Ethanol, 2-(methylphenylamino)-

C9H13NO

收率 89%

PROCEDURE

实验过程

Prepared in the manner of Example 23 except ethyl N-methyl-N-phenylglycinate was substituted for ethyl N-methyl-N-{4-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]phenyl}glycinate. Purification by flash chromatography (1:1 hexanes/EtOAc) afforded the title compound as a yellow oil (89%). MS (ES+) m/z 152 (MH+).

WORKUP

后处理

  1. customPurification by flash chromatography (1:1 hexanes/EtOAc)