Hexylamine → HCID 21977479, compound

HRID 2184283Notes

Reaction equation

HRID 2184283 reaction equation
[C:1]([OH:8])(=O)[CH2:2][CH2:3][C:4]([CH3:6])=O.[CH2:9]([NH2:15])[CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>O>[CH3:6][CH:4]1[N:15]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[C:1](=[O:8])[CH2:2][CH2:3]1

Participants

4

Reactant 2

HCID 8102HexylamineHCID 11579Levulinic Acid

Product 1

HCID 21977479HCID 21977479, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

The feedstock used in examples 31 through 38 was 30% of the ammonium salt of levulinic acid, 26% hexylamine, and 24% water by weight. The temperature and pressure of the reactions were maintained at 150° and 6.9 MPa. Water was used as the solvent medium for the reactions. The results are set forth in the following table.

Workup

  1. temperatureThe temperature and pressure of the reactions were maintained at 150°

Sources & evidence

ORD record
ord-01e28452b4464a30aa4c1707298549c2
Source dataset
uspto-grants-2005_05
Patent number
US06900337B2

Reaction notes

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