Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | Levulinic Acid | HCID 11579 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 11447171 | HCID 11447171 | — |
Reaction Steps
The feedstock used in examples 39 through 77, except for example 40, was 20% of the ammonium salt of levulinic acid, 40% octylamine, and 40% water, by weight. For the reaction in example 40, the weight ratio of the feedstock was 30% of the ammonium salt of levulinic acid, 30% octylamine, and 40% water. The temperature and pressure of the reactions were maintained at 150° C. and 6.9 MPa. Water was used as the solvent medium for the reactions. The results are set forth in the following table.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06900337B2 |
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| Source dataset | uspto-grants-2005_05 |
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| ORD ID | ord-ac6ef117749d43788946504a4abf437a |
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| Source note | uspto-grants-2005_05 |
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