Octylamine → HCID 11447171, compound

HRID 2184284Notes

Reaction equation

[C:1]([OH:8])(=O)[CH2:2][CH2:3][C:4]([CH3:6])=O.[CH2:9]([NH2:17])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>O>[CH3:6][CH:4]1[N:17]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[C:1](=[O:8])[CH2:2][CH2:3]1

Participants

Conditions

Temperature: 150 °C

Procedure

The feedstock used in examples 39 through 77, except for example 40, was 20% of the ammonium salt of levulinic acid, 40% octylamine, and 40% water, by weight. For the reaction in example 40, the weight ratio of the feedstock was 30% of the ammonium salt of levulinic acid, 30% octylamine, and 40% water. The temperature and pressure of the reactions were maintained at 150° C. and 6.9 MPa. Water was used as the solvent medium for the reactions. The results are set forth in the following table.

Workup

customFor the reaction in example 40

Sources & evidence

ORD record: ord-ac6ef117749d43788946504a4abf437a
Source dataset: uspto-grants-2005_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06900337B2

Reaction notes

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