HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 69289483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 3-{4-[(3-Fluorophenyl)methoxy]phenyl}prop-2-enoyl chloride | HCID 71377679 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69289483 | HCID 69289483 | 72% |
Reaction Steps
The title compound is prepared in analogy to example 9, using crude 3-[4-(3-fluoro-benzyloxy)-phenyl]-acryloyl chloride and a 2 M solution of ethylamine in dichloromethane. Colorless solid. Yield=72%. MS: m/e=300.3 (M++H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900354B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-d5b74875d5c749fd88ee47c08b485d1b |
| Source note | uspto-grants-2005_05 |