HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile, 3-(bromomethyl)- → 3-{4-[(3-Cyanophenyl)methoxy]phenyl}-N-methylprop-2-enamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile, 3-(bromomethyl)- | HCID 97249 | — |
| Reactant | 3-(4-Hydroxyphenyl)-N-methylprop-2-enamide | HCID 54400570 | — |
| Product | 3-{4-[(3-Cyanophenyl)methoxy]phenyl}-N-methylprop-2-enamide | HCID 69291715 | 75% |
Reaction Steps
The title compound is prepared in analogy to example 11 b) from 3-(4-hydroxy-phenyl)-N-methyl-acrylamide and 3-bromomethyl-benzonitrile. Yield=75%. Colorless solid. MS: m/e=293.2 (M++H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900354B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-130f55bbee4e4e5b800fdf98d91a15bc |
| Source note | uspto-grants-2005_05 |