HCID 22476587, compound → HCID 22476602, compound

Participants

Reaction Steps

[(Methylethyl)sulfonyl][2-(phenylmethoxy)cyclohexyl]amine (11.41 g, 36.6 mmol) and 10% palladium on carbon (1.40 g) were combined in ethanol (300 mL) and placed on the power shaker under a hydrogen atmosphere at 60 psi's overnight. The solution was then filtered over a Celite® mat and the resulting filtrate was concentrated under reduced vacuum to yield the intermediate title compound (6.78 g, 84%) as a white solid. Ion Spray M.S. 222.1 (M*+1). Calculated for C9H19NO3S: Theory: C 48.84, H 8.65, N 6.32. Found: C 49.10, H 8.84, N 6.42.

Provenance & Evidence