1,3-Dibromobutane → HCID 22457550, compound

HRID 2184717Notes

Reaction equation

HRID 2184717 reaction equation
[Br:1][CH2:2][CH2:3][CH:4]([Br:6])[CH3:5].[CH2:7]1[N:12]2[CH2:13][CH2:14][N:9]([CH2:10][CH2:11]2)[CH2:8]1>C(#N)C>[Br-:1].[Br:6][CH:4]([CH3:5])[CH2:3][CH2:2][N+:9]12[CH2:14][CH2:13][NH+:12]([CH2:11][CH2:10]1)[CH2:7][CH2:8]2.[Br-:1]

Participants

4

Reactant 2

HCID 78891,3-DibromobutaneHCID 9237Dabco

Product 1

HCID 22457550HCID 22457550, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

1,3-Dibromobutane (2.15 g, 1.2 ml, 10 mmol) was dissolved in acetonitrile (2 ml). DABCO (1.23 g, 11 mmol) was added. The reaction mixture was heated at 65° under nitrogen for 2 hr. The acetonitrile was removed under reduced pressure to give a white solid as the product.

Workup

  1. temperatureThe reaction mixture was heated at 65° under nitrogen for 2 hr
  2. customThe acetonitrile was removed under reduced pressure
  3. customto give a white solid as the product

Sources & evidence

ORD record
ord-0f5953375fe14bd3bf74e26144cdf6ed
Source dataset
uspto-grants-2002_06
Patent number
US06399597B1

Reaction notes

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