2,2-Diphenylacetyl chloride → HCID 10269945, compound
Reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH2:7][C:8]([F:11])([F:10])[F:9])[N:6]=1.[C:12]1([CH:18]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[C:19](Cl)=[O:20])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:22]1([CH:18]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)[C:19]([NH:1][C:2]2[N:3]=[N:4][N:5]([CH2:7][C:8]([F:9])([F:11])[F:10])[N:6]=2)=[O:20])[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1Participants
3
Procedure
The title compound, white solid, m.p. 146-148 and MS: (neg. ions): m/e=360.0 (M+−H) was prepared in accordance with the general method of example 1 from 5-amino-2-(2,2,2-trifluoroethyl)-2H-tetrazole and diphenylacetyl chloride.
Sources & evidence
- ORD record
- ord-b3c44da485dd48ed98174bad63bd9734
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06399641B1
Reaction notes
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