2,2-Diphenylacetyl chloride → HCID 9880526, compound
Reaction equation
[NH2:1][C:2]1[N:3]=[N:4][N:5]([CH:7]([F:9])[F:8])[N:6]=1.[C:10]1([CH:16]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[C:17](Cl)=[O:18])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[F:8][CH:7]([F:9])[N:5]1[N:4]=[N:3][C:2]([NH:1][C:17](=[O:18])[CH:16]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[N:6]1Participants
3
Procedure
The title compound, white solid, m.p. 143-145° and MS: (neg. ions): m/e=328.1 (M+−H) was prepared in accordance with the general method of example 1 from 5-amino-2-difluoromethyl-2H-tetrazole and diphenylacetyl chloride.
Sources & evidence
- ORD record
- ord-55ead17a8e7342e9a2cbcbffdb88cd5c
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06399641B1
Reaction notes
Loading…