HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Acetylsulfanilyl chloride → N-{4-[Methyl-(1-methylpyrrolidin-3-yl)sulfamoyl]phenyl}acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Acetylsulfanilyl chloride | HCID 8481 | — |
| Reactant | N,1-dimethylpyrrolidin-3-amine | HCID 2758520 | — |
| Product | N-{4-[Methyl-(1-methylpyrrolidin-3-yl)sulfamoyl]phenyl}acetamide | HCID 22460074 | — |
Reaction Steps
4-Acetylaminobenzenesulfonyl chloride and methyl-(1-methylpyrrolidin-3-yl)amine are reacted according to the method described in Example 10, intermediate 2. The title compound obtained in the form of a slightly yellowish solid can be reacted further without further purification. (MS-ES+: 312.1; LCMS Rt=0.698 min)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06399824B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-ed4d82b57f3a4d8b845cb58b2f035ba4 |
| Source note | uspto-grants-2002_06 |