HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenol → HCID 53661325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenol | HCID 9743 | — |
| Reactant | 4-Chlorobutyryl chloride | HCID 78370 | — |
| Product | HCID 53661325 | HCID 53661325 | — |
Reaction Steps
4-Chlorobutyrylchloride (35.3 g) was added to 3-fluorophenol (25 g). This mixture was stirred during 48 h at room temperature. After the reaction was completed the product was purified by vacuo-destillation. Yield: 35,3 g (b.p. 106° C. 3 mmHg) of 4-chloro-butanoic acid 3-fluorophenyl ester as a white oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403573B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-0ef28005a6694d8da1899c0fe5492031 |
| Source note | uspto-grants-2002_06 |