Propylamine → HCID 60208168, compound

HRID 2185668Notes

Reaction equation

HRID 2185668 reaction equation
[CH2:1]([O:8][C:9]([N:11]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH2:13][C@H:12]1[C:20]([OH:22])=O)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:23]([NH2:26])[CH2:24][CH3:25]>>[CH2:23]([NH:26][C:20]([C@@H:12]1[CH2:13][C:14]2[C:19](=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:11]1[C:9]([O:8][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)=[O:10])=[O:22])[CH2:24][CH3:25]

Participants

3

Reactant 2

HCID 7852PropylamineHCID 6932064HCID 6932064, compound

Product 1

HCID 60208168HCID 60208168, compound

Procedure

The process is performed as in Example 14 a), starting with N-benzyloxycarbonyl-2(S)-indolinecarboxylic acid prepared as in Example 16 a) and n-propylamine. A white solid is obtained, which is recrystallized from CCl4.

Workup

  1. customA white solid is obtained
  2. customwhich is recrystallized from CCl4

Sources & evidence

ORD record
ord-c2b3840229fb44d9a36e9029d2d6ca2b
Source dataset
uspto-grants-2002_06
Patent number
US06403561B1

Reaction notes

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