HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14691534, compound → HCID 23313846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14691534 | HCID 14691534 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23313846 | HCID 23313846 | — |
Reaction Steps
Ethyl 3,3-dimethyl-3H-indole-2-carboxylate (4.00 g, 18.4 mmol) was dissolved in ethanol (20 ml) and activated palladium-on-charcoal (0.5 g) was then added to this solution. This mixture was hydrogenated for five hours. After filtration in order to remove the catalyst, the filtrate was dried (MgSO4) and the solvent removed in order to give a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403561B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-aa28a24f8b2e4f17b2040e653840eb2d |
| Source note | uspto-grants-2002_06 |