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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2185682Generated: October 29, 2026

HCID 14691534, compound → HCID 23313846, compound

https://huagongshe.com/reaction/2185682

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14691534HCID 14691534—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 23313846HCID 23313846—

Reaction Steps

Ethyl 3,3-dimethyl-3H-indole-2-carboxylate (4.00 g, 18.4 mmol) was dissolved in ethanol (20 ml) and activated palladium-on-charcoal (0.5 g) was then added to this solution. This mixture was hydrogenated for five hours. After filtration in order to remove the catalyst, the filtrate was dried (MgSO4) and the solvent removed in order to give a brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403561B1
Source datasetuspto-grants-2002_06
ORD IDord-aa28a24f8b2e4f17b2040e653840eb2d
Source noteuspto-grants-2002_06