HCID 86587267, compound → HCID 4715066, compound

HRID 2185688Notes

Reaction equation

HRID 2185688 reaction equation
[N:1]([C:4](=[CH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[O:16][CH2:17][CH3:18])[C:5]([O:7][CH3:8])=[O:6])=[N+]=[N-]>C1(C)C=CC=CC=1>[CH2:17]([O:16][C:11]1[CH:12]=[CH:13][CH:14]=[C:15]2[C:10]=1[CH:9]=[C:4]([C:5]([O:7][CH3:8])=[O:6])[NH:1]2)[CH3:18]

Participants

3

Reactant 1

HCID 86587267HCID 86587267, compound

Product 1

HCID 4715066HCID 4715066, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Methyl 2-azido-3-(2-ethoxyphenyl)propenoate (2.061 g, 10 mmol) was suspended in toluene (500 ml) and the mixture was refluxed for three hours and then maintained at room temperature overnight. The solids were collected by filtration in order to give the desired product in the form of a yellow solid.

Workup

  1. temperaturethe mixture was refluxed for three hours
  2. filtrationThe solids were collected by filtration in order

Sources & evidence

ORD record
ord-eb80e3a9995f4dab9d355bb5e28dff4c
Source dataset
uspto-grants-2002_06
Patent number
US06403561B1

Reaction notes

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