HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86587267, compound → HCID 4715066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86587267 | HCID 86587267 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 4715066 | HCID 4715066 | — |
Reaction Steps
Methyl 2-azido-3-(2-ethoxyphenyl)propenoate (2.061 g, 10 mmol) was suspended in toluene (500 ml) and the mixture was refluxed for three hours and then maintained at room temperature overnight. The solids were collected by filtration in order to give the desired product in the form of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403561B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-eb80e3a9995f4dab9d355bb5e28dff4c |
| Source note | uspto-grants-2002_06 |