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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2185692Generated: October 29, 2026

HCID 73886677, compound → HCID 22451293, compound

https://huagongshe.com/reaction/2185692

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 73886677HCID 73886677—
SolventTolueneHCID 1140—
ProductHCID 22451293HCID 22451293—

Reaction Steps

Ethyl 2-azido-3-(2,3-dimethoxyphenyl)propeneoate (4.0 g, 144 mmol) was suspended in toluene (120 ml) and the mixture was refluxed for three hours and then cooled and stirred at room temperature overnight. The solids were collected by filtration in order to give the product in the form of a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06403561B1
Source datasetuspto-grants-2002_06
ORD IDord-a359b80643df44f9b54ebc4c8ebaf0c9
Source noteuspto-grants-2002_06