HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 73886677, compound → HCID 22451293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 73886677 | HCID 73886677 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22451293 | HCID 22451293 | — |
Reaction Steps
Ethyl 2-azido-3-(2,3-dimethoxyphenyl)propeneoate (4.0 g, 144 mmol) was suspended in toluene (120 ml) and the mixture was refluxed for three hours and then cooled and stirred at room temperature overnight. The solids were collected by filtration in order to give the product in the form of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403561B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-a359b80643df44f9b54ebc4c8ebaf0c9 |
| Source note | uspto-grants-2002_06 |