HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22451271, compound → HCID 77752253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22451271 | HCID 22451271 | — |
| Solvent | Butylamine | HCID 8007 | — |
| Product | HCID 77752253 | HCID 77752253 | — |
Reaction Steps
Methyl 5-chloroindoline-2(R/S)-carboxylate (0.63 g, 3 mmol) was dissolved in butylamine (25 ml) and refluxed for 4 h. The excess amine was removed and the residue was crystallized from ether to give a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403561B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-57d20b3d7f1e4e0e88619c851ce551d0 |
| Source note | uspto-grants-2002_06 |