HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinemethanamine → HCID 22452170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Reactant | HCID 22452283 | HCID 22452283 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 22452170 | HCID 22452170 | 44.5% |
Reaction Steps
In xylene, 2-ethoxycarbonylmethyl-6-(4-methoxyphenyl)-4-methylcarbamoyl-2H-pyridazin-3-one and 2-(aminomethyl)pyridine were refluxed at 150° C. for 7 hours. Post-treatments were conducted as in Example 47-(2), whereby the title compound was obtained in a yield of 44.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403586B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-2aaf15aae15541928d8bec0b7ad257de |
| Source note | uspto-grants-2002_06 |