HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 22452221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | HCID 22452283 | HCID 22452283 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22452221 | HCID 22452221 | 91% |
Reaction Steps
In methanol, 2-ethoxycarbonylmethyl-6-(4-methoxyphenyl)-4-methylcarbamoyl-2H-pyridazin-3-one and 2-aminoethanol were heated under reflux for 4 hours. Post-treatments were conducted as in Example 43, whereby the title compound was obtained in a yield of 91.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403586B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-a308a2fba97147c18a11a908186803df |
| Source note | uspto-grants-2002_06 |