HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Pyridinemethanamine → HCID 22452216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Reactant | HCID 22452200 | HCID 22452200 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 22452216 | HCID 22452216 | 84.2% |
Reaction Steps
In xylene, 2-cyclopropylmethyl-4-ethoxycarbonyl-6-(4-methoxyphenyl)-2H-pyridazin-3-one and 2-(aminomethyl)pyridine were reacted at 140° C. for 1 hour. Post-treatments were conducted as in Example 58-(3), whereby the title compound was obtained in a yield of 84.2%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403586B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-ba6df2107d704ec8ba30fcef0457d96f |
| Source note | uspto-grants-2002_06 |