HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 22452646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 22452685 | HCID 22452685 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22452646 | HCID 22452646 | — |
Reaction Steps
A stirred mixture of 3-cyano-2-methoxy-5,6,7,8-tetrahydro-1-naphthalenecarboxylic acid (0.110 g, 0.476 mmol) and dry CH2Cl2 (2 mL) was treated with oxalyl chloride (51.9 μl) and dry N,N-dimethylformanide (˜5 μL) at ambient temperature. After 2.0 h, the solvent was evaporated in vacuo. The residue was dissolved in dry CH2Cl2 and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403601B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-2a5e11cac70d45029db67aef14b6663c |
| Source note | uspto-grants-2002_06 |