HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69892168, compound → HCID 86586189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69892168 | HCID 69892168 | — |
| Solvent | N,N-Dimethylaniline | HCID 949 | — |
| Product | HCID 86586189 | HCID 86586189 | 179.8% |
Reaction Steps
0.89 g of 6-t-butyl-5-(2-methyl-2-propenyloxy)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane was dissolved in 3 ml of dimethylaniline and the solution was treated in the same manner as in Example 8-2) to give 0.80 g of 6-t-butyl-5-hydroxy-4-(2-methyl-2-propenyl)-2,3-dihydrobenzofuran-2-spiro-1′-cycloheptane as a colorless oil (yield 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403639B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-a93e7c2cb3a64fc68c3eecc684e761aa |
| Source note | uspto-grants-2002_06 |