HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,5-Diisopropylphenyl)boronic acid → 1-tert-Butyl-4,4-dimethyl-3,4-dihydro-naphthalen-7-boronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,5-Diisopropylphenyl)boronic acid | HCID 11543001 | — |
| Reactant | 6-Bromo-4-tert-butyl-1,1-dimethyl-1,2-dihydronaphthalene | HCID 15896019 | — |
| Product | 1-tert-Butyl-4,4-dimethyl-3,4-dihydro-naphthalen-7-boronic acid | HCID 22456165 | — |
Reaction Steps
Employing the procedure used for the preparation of 3,5-diisopropylphenylboronic acid (Compound 2), 1-tert-butyl-4,4-dimethyl-3,4-dihydro-7-bromonaphthalene (Compound 16) was converted to the title compound. The resulting crude product was used in the next step without further purification. 1-tert-butyl-4,4-dimethyl-3,4-dihydro-7-bromonaphthalene (Compound 16) can be obtained in accordance with the disclosure of U.S. Pat. No. 5,741,896, incorporated herein by reference.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06403638B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-3f0b104346384be2866365c0918ca686 |
| Source note | uspto-grants-2002_06 |