反应详情

In a 200 ml autoclave were charged 8.50 g (29.5 mmol) of ethyl (R)-4-azido-3-hexanoyloxybutyrate, 0.20 g of 5% Pd—C, and 16 ml of ethyl acetate, and the mixture was stirred at room temperature under a hydrogen pressure of 1000 KPa. for 7 hours. The catalyst was removed for concentration to give 7.07 g (87%) of the title compound.

1. customThe catalyst was removed for concentration