1-Bromo-2-propanol → Propylene Oxide
Reaction equation
[CH2:1]([Br:5])[CH:2]([OH:4])[CH3:3]>CC(C)=O>[CH2:1]([Br:5])[CH:2]([OH:4])[CH3:3].[CH2:1]1[O:4][CH:2]1[CH3:3]Participants
4
Reactant 1
Product 2
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 100 °C
Procedure
Propylene bromohydrin (1.00 ml/hour) and helium (2.0 ml/minute) were passed through a reactor that was packed with 3.0000 gram M1, which was heated to 100° C. Within the first 2 hours, an average propylene bromohydrin conversion of 35%, with 50% propylene oxide average selectivity and 50% acetone selectivity was obtained. In the second hour, only propylene oxide was obtained.
Sources & evidence
- ORD record
- ord-2ce9ccbd0c414121b335ea1b6027e01f
- Source dataset
- uspto-grants-2002_06
- Patent number
- US06403840B1
Reaction notes
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