Hydrochloric Acid → HCID 131723309, compound

Participants

Reaction Steps

BocNle-pNA (prepared in 1 (1); 2.96 g) was dissolved into a solution of 4N—HCl in dioxane (30 ml). After stirring the obtained solution for 1 hour at room temperature, dioxane was distilled off under reduced pressure and then by adding toluene (30 ml). The reaction mixture was crystallized in ether to give Nle-pNA.HCl (2.08 g).

Provenance & Evidence