HCID 18669803, compound → HCID 18475148, compound

Participants

Reaction Steps

3.55 g (53.8 mmol) of lithium isopropoxide was added to 6.25 g (53.8 mmol) of dimethylaluminum isopropoxide dissolved in diethyl ether and stirred for a day. The resulting mixture was distilled under a reduced pressure to remove the solvent and the resulting solid residue was sublimed under a vacuum at 110° C. to obtain 8.98 g (49.3 mmol; 92% yield) of the title compound in the form of a white solid.

Provenance & Evidence