HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18475662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 18475631 | HCID 18475631 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18475662 | HCID 18475662 | — |
Reaction Steps
Methanesulphonyl chloride (27 ul) was added to 1-(3-aminophenyl)-3-quinolin-4-ylurea (0.08 g) in dichloromethane (25 ml) containing triethylamine (48 ul) and stirred for 16 h. The precipitate that formed was separated by filtration, washed with tetrahydrofuran and diethyl ether and dried to give the title compound (0.081 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06410529B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-24495b2207bf4a56aa0f5e27da2d30c9 |
| Source note | uspto-grants-2002_06 |