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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2187494Generated: October 30, 2026

Hydrochloric Acid → HCID 70032107, compound

https://huagongshe.com/reaction/2187494

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantAR-A000002HCID 9846516—
SolventDiethyl EtherHCID 3283—
SolventTetrahydrofuranHCID 8028—
ProductHCID 70032107HCID 70032107—

Reaction Steps

(R)-N-[5-Methyl-8-(4-methylpiperazin-1-yl)-1,2,3,4-tetrahydro-2-naphthyl]-4-morpholinobenzamide (100 mg, 0.22 mmol) was dissolved in anhydrous tetrahydrofuran (15 mL) and HCl in anhydrous diethyl ether (4 M) was added dropwise until the solution was acidic. The white precipitate was filtered and washed with diethyl ether to give the title compound as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06410532B1
Source datasetuspto-grants-2002_06
ORD IDord-fa11ec04b3c6464280fa45530c533d25
Source noteuspto-grants-2002_06