Butyl iodide → HCID 18476309, compound

HRID 2187641Notes

Reaction equation

HRID 2187641 reaction equation
[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[C:4]([C:12]([O:14][CH2:15][CH3:16])=[O:13])[C:3]=1[OH:17].[CH2:18](I)[CH2:19][CH2:20][CH3:21]>>[Br:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[C:4]([C:12]([O:14][CH2:15][CH3:16])=[O:13])[C:3]=1[O:17][CH2:18][CH2:19][CH2:20][CH3:21]

Participants

3

Reactant 2

HCID 10962Butyl iodideHCID 18476329HCID 18476329, compound

Product 1

HCID 18476309HCID 18476309, compound

Procedure

The intermediate was prepared from ethyl 4-bromo-3-hydroxynaphthalen-2-carboxylate and butyl iodide in almost quantitative yield and used for the next step without further purification.

Workup

  1. customused for the next step without further purification

Sources & evidence

ORD record
ord-fa39e74398ad43b6a7cafd5b8eedb04f
Source dataset
uspto-grants-2002_06
Patent number
US06410562B1

Reaction notes

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