HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18475842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 18475884 | HCID 18475884 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18475842 | HCID 18475842 | — |
Reaction Steps
A solution of 1-(tert-butoxycarbonylamino)-7-(tert-butyldiphenylsilyloxy)naphthalene, as described above in Step B, (1.54 g, 3.09 mmol) in EtOAc (80 mL) and Et2O (20 mL) at ambient temperature was saturated with HCl (g). After 1 hr, the mixture was concentrated in vacuo to yield the desired product as a pale solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06410534B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-07d69559853b46c799200cc871c93321 |
| Source note | uspto-grants-2002_06 |