HRID2188080

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13819

Silane, chlorotriethyl-

C6H15ClSi

HCID82566

2-Chloro-N,N-diethylbenzamide

C11H14ClNO

PRODUCTS

生成物

结构：CCN(CC)C(=O)c1c(Cl)cccc1[Si](CC)(CC)CC

HCID18630182

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to General Method A from the compound of Example e and 1.4 eq chlorotriethylsilane. Purification by HPLC with 1:19 ethyl acetate/hexanes gave 6.0 g of the desired product as a clear oil, a 92% yield.

WORKUP

后处理

customThe title compound was prepared
customPurification by HPLC with 1:19 ethyl acetate/hexanes